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Controlled substance report(2)LONG BEACH POLICE DEPARTMENT FORENSIC SCIENCE SERVICES DIVISION CRIME LABORATORY – CONTROLLED SUBSTANCE UNIT CONTROLLED SUBSTANCES ANALYSIS REPORT 1400 Canal Ave., Long Beach, CA 90813 VICTIM/SUSPECT: Ball, James BOOKING #: 5094068 DR #: 170054269 EVIDENCE RECEIVED FROM: Controlled Substance Lab DATE RECEIVED: 09/08/2017 REQUESTED BY: DIS This laboratory report contains results and interpretations: Item 3 – Tag 887184 One sealed brown bag containing a metal cooking pan, a piece of foil, and a plastic dish, each containing what appears to be cooked residue. I found one green leaf inside the pan. I examined the leaf and determined that it is from a marijuana plant. I found residue of what appears to be cake from a cooked brownie on the pan. I tested this cake and found no cannabinoids. I found grease deposits inside the pan. I tested this deposit and found no cannabinoids. I found one green leaf on the side of the foil containing cooked residue. I examined the leaf and determined that it is from a marijuana plant. I found residue of what appears to be cake from a cooked brownie on the foil. I tested this cake and determined that it contains tetrahrdyocannabinol. I found grease deposits on the foil. I tested this deposit and found no cannabinoids. I found several small portions of leaves on the dish. I tested one leaf and determined that it contains marijuana. I found grease deposits on the dish. I tested this deposit and found no cannabinoids. Disposition: The evidence was returned to the Controlled Substance Laboratory following analysis. DATE OF REPORT: 09/13/2017 CRIMINALIST II: TECHNICAL REVIEW BY: ADMINISTRATIVE REVIEW BY: An ASCLD/LAB – International Accredited Testing Laboratory Since October 16, 2014 (ALI-360-T) Page 1 of 13 170054269 1-13 Gregory Gossage 7885 2017.09.13 13:18:12 -07'00' JJ10338 2017.09.13 13:56:11 -07'00'JJ10338 2017.09.13 13:56:34 -07'00' LONG BEACH POLICE DEPARTMENT CONTROLLED SUBSTANCE ANALYSIS WORKSHEET DR # 170054269 Tag # 887184 One sealed box (PT-10745); Received from controlled substance lab on 09/08/2017 Date analysis started: 09/08/2017 Item 3 – One sealed brown bag containing a metal cooking pan containing what appears to be cooked residue. I found residue of what appears to be cake from a cooked brownie on the pan. I found one green leaf on the pan. I tested a portion of it. Duquenois / Levine (expires 05/08/2019 lot# AB050817) – purple / purple (hydrochloric acid lot# 146345 no expiration; chloroform lot# A0350128 no expiration) cystolithic / glandular hairs– positive for marijuana (American Optical Forty s/n 199806 @ 15x magnification) GC/MS analysis – tetrahydrocannabinol; blanks after each sample and standard were negative. Analysis of grease deposit and cake taken from pan; GC/MS analysis – negative for cannabinoids; blanks after each sample and standard were negative. Close - up Date analysis completed: 09/13/2017 Notes by G. Gossage 7885 Page 2 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184p3.D Operator : Acquired : 13 Sep 2017 12:10 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 leaf from pan Misc Info : in methanol lot# 155201-1 Vial Number: 20 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 50000 100000 150000 200000 250000 300000 350000 400000 450000 500000 550000 600000 Time--> Abundance TIC: 887184p3.D\data.ms 5.248 7.374 7.929 8.294 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 330 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 m/z--> Abundance Average of 8.294 to 8.323 min.: 887184p3.D\data.ms (-)299 314 231 271 243 258 174 19391201 217115811281471071656755 28515718313720999 Page 3 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184p.D Operator : Acquired : 13 Sep 2017 9:16 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 cake from pan Misc Info : in ethanol lot# 156617 Vial Number: 25 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 Time--> Abundance TIC: 887184p.D\data.ms .156 2.213 2.379 3.613 3.773 3.888 4.002 4.082 6.357 6.951 7.374 9.146 9.517 12.072 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 0 200 400 600 800 1000 1200 1400 1600 1800 2000 2200 2400 m/z--> Abundance Average of 12.049 to 12.095 min.: 887184p.D\data.ms (-)386 275 145107 301 95 81 36821355353 159119133 255 67 231 173 199187 326 343314 415 429287243 Page 4 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184p2.D Operator : Acquired : 13 Sep 2017 11:00 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 from pan Misc Info : in ethanol lot# 156617 Vial Number: 22 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 2000 4000 6000 8000 10000 12000 14000 16000 Time--> Abundance TIC: 887184p2.D\data.ms 6.254 6.368 6.968 6.997 7.368 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 0 50 100 150 200 250 300 350 400 450 500 550 600 650 m/z--> Abundance Average of 7.357 to 7.386 min.: 887184p2.D\data.ms (-)207 414 303 105 119 32914555 3968116328113395 69 381 191 255177 341 355 221231 267 Page 5 of 13 170054269 LONG BEACH POLICE DEPARTMENT CONTROLLED SUBSTANCE ANALYSIS WORKSHEET DR # 170054269 Tag # 887184 - continued - Date analysis started: 09/08/2017 The sealed brown bag also contained a piece of aluminum foil containing what appears to be cooked residue. I found residue of what appears to be cake from a cooked brownie on the foil. I found one green leaf on the foil. I tested a portion of it. Duquenois / Levine (expires 05/08/2019 lot# AB050817) – purple / purple (hydrochloric acid lot# 146345 no expiration; chloroform lot# A0350128 no expiration) cystolithic / glandular hairs– positive for marijuana (American Optical Forty s/n 199806 @ 15x magnification) Analysis of cake found on the foil; GC/MS analysis – tetrahydrocannabinol; blanks after each sample and standard were negative. Analysis of grease found on the foil; GC/MS analysis – negative for cannabinoids; blanks after each sample and standard were negative. Close - up Date analysis completed: 09/13/2017 Notes by G. Gossage 7885 Page 6 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184f3.D Operator : Acquired : 13 Sep 2017 12:45 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 leaf from foil Misc Info : in methanol lot# 155201-1 Vial Number: 19 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 50000 100000 150000 200000 250000 300000 350000 400000 450000 500000 550000 600000 650000 Time--> Abundance TIC: 887184f3.D\data.ms 7.380 8.294 8.557 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 m/z--> Abundance Average of 8.283 to 8.323 min.: 887184f3.D\data.ms (-)299 314 231 271 243 258 174 19391 217201115811281076716514755 28515718513620925199 Page 7 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184f.D Operator : Acquired : 13 Sep 2017 9:50 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 cake from foil Misc Info : in ethanol lot# 156617 Vial Number: 24 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 Time--> Abundance TIC: 887184f.D\data.ms 133 2.213 2.270 2.408 2.459 2.550 2.711 2.813 3.065 3.305 3.408 3.494 3.631 4.208 5.054 6.363 6.443 6.677 6.831 6.957 7.094 7.380 7.711 8.294 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 330 340 350 360 0 100 200 300 400 500 600 700 800 900 1000 1100 m/z--> Abundance Average of 8.289 to 8.300 min.: 887184f.D\data.ms (-)299 314 231 243 271 258 207 91557967 107 221121187147163177 343282135 327 Page 8 of 13 170054269 File :C:\msdchem\1\DATA\170913\THC2.D Operator : Acquired : 13 Sep 2017 8:41 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: THC std lot# 60H4030 Misc Info : in methanol lot# 155201-1 Vial Number: 86 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 5000000 1e+07 1.5e+07 2e+07 2.5e+07 3e+07 Time--> Abundance TIC: THC2.D\data.ms 8.323 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 m/z--> Abundance Average of 8.306 to 8.328 min.: THC2.D\data.ms (-)299 314 231 271 243 258 193174 2172019111512816514710781 285675515718313720999 32 Page 9 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184f2.D Operator : Acquired : 13 Sep 2017 11:35 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 from foil Misc Info : in ethanol lot# 156617 Vial Number: 21 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 Time--> Abundance TIC: 887184f2.D\data.ms 116 2.270 3.070 3.305 4.808 4.911 5.534 6.140 6.180 6.254 6.362 6.614 6.843 6.911 6.940 7.048 7.374 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 0 50 100 150 200 250 300 350 400 m/z--> Abundance Average of 7.357 to 7.397 min.: 887184f2.D\data.ms (-)207 414 145 13395 3295530381107 396119163191 69 283 355341 381 255 177 267231 429 Page 10 of 13 170054269 LONG BEACH POLICE DEPARTMENT CONTROLLED SUBSTANCE ANALYSIS WORKSHEET DR # 170054269 Tag # 887184 - continued - Date analysis started: 09/08/2017 The sealed brown bag also contained a clear plastic dish containing what appears to be cooked residue and green plant material. I tested one leaf taken from the dish. Duquenois / Levine (expires 05/08/2019 lot# AB050817) – purple / purple (hydrochloric acid lot# 146345 no expiration; chloroform lot# A0350128 no expiration) cystolithic / glandular hairs– positive for marijuana (American Optical Forty s/n 199806 @ 15x magnification) Analysis of grease deposit taken from the dish. GC/MS analysis – negative for cannabinoids; blanks after each sample and standard were negative. Date analysis completed: 09/13/2017 Notes by G. Gossage 7885 Page 11 of 13 170054269 File :C:\msdchem\1\DATA\170913\887184d.D Operator : Acquired : 13 Sep 2017 10:26 using AcqMethod THC.M Instrument : sn MS 2845 GC 8100 Sample Name: 887184 item 3 from dish Misc Info : in ethanol lot# 156617 Vial Number: 23 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 0 2000 4000 6000 8000 10000 12000 14000 16000 Time--> Abundance TIC: 887184d.D\data.ms 2.990 5.368 5.985 6.100 6.191 6.254 6.351 6.768 6.843 6.905 7.368 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 0 50 100 150 200 250 300 350 400 450 m/z--> Abundance Average of 7.357 to 7.391 min.: 887184d.D\data.ms (-)207 414 10781 95 119 191 303 55 147 15969133 329 396281255 341 381177 429231355 Page 12 of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age 13 of 13 170054269